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1.
ACS Biomater Sci Eng ; 10(4): 2100-2115, 2024 Apr 08.
Artigo em Inglês | MEDLINE | ID: mdl-38502729

RESUMO

Over the past decade, bone tissue engineering has been at the core of attention because of an increasing number of implant surgeries. The purpose of this study was to obtain coatings on titanium (Ti) implants with improved properties in terms of biomedical applications and to investigate the effect of ultrasound (US) on these properties during the micro-arc oxidation (MAO) process. The influence of various process parameters, such as time and current density, as well as US mode, on the properties of such coatings was evaluated. Novel porous calcium-phosphate-based coatings were obtained on commercially pure Ti. Their microstructure, chemical composition, topography, wettability, nanomechanical properties, thickness, adhesion to the substrate, and corrosion resistance were analyzed. In addition, cytocompatibility evaluation was checked with the human osteoblasts. The properties of the coatings varied significantly, depending on applied process parameters. The US application during the MAO process contributes to the increase of coating thickness, porosity, roughness, and skewness, as well as augmented calcium incorporation. The most advantageous coating was obtained at a current of 136 mA, time 450 s, and unipolar rectangular US, as it exhibits high porosity, adequate wettability, and beneficial skewness, which enabled increased adhesion and proliferation of osteoblasts during in vitro studies. Finally, the conducted research demonstrated the influence of various UMAO process parameters, which allowed for the selection of appropriate Ti implant modification for specific biomedical utilization.


Assuntos
Cálcio , Materiais Revestidos Biocompatíveis , Humanos , Materiais Revestidos Biocompatíveis/farmacologia , Materiais Revestidos Biocompatíveis/química , Cálcio/química , Engenharia Biomédica , Oxirredução , Molhabilidade
2.
Materials (Basel) ; 14(6)2021 Mar 16.
Artigo em Inglês | MEDLINE | ID: mdl-33809528

RESUMO

During the low plasticity burnishing process of soft materials such as carbon steel with a hardness of up to 40 HRC (Rockwell grade) a raised structure of the material known as the Jumping Wave forms in front of the tool roll. This phenomenon significantly disturbs the burnishing process, but is very poorly described in the literature. This article presents studies of this phenomenon on the example of burnished 1.0562 steel. The research concerns the changes in the surface structure of the processed material as well as changes in the structure of the material during this process. The research shows changes in the geometric structure of the surface made in the 3D system and their parametric description. Moreover, the work presents an analysis of the metallographic structure in the tool zone. The research showed occurrence of material slippages in the wave in front of the tool, which creates an additional structure on the surface. These tests make it possible to better understand the process of changes that take place in the surface layer of the processed element in the low plasticity burnishing process.

3.
Materials (Basel) ; 12(2)2019 Jan 09.
Artigo em Inglês | MEDLINE | ID: mdl-30634434

RESUMO

This article represents the results of testing the surface condition of shafts manufactured by the burnishing process. The shafts with a hardness of approximately 62 HRC (Rockwell C). were burnished with a ceramic ball (Si3N4), where the force range was controlled by the means of a hydraulic system. The machining process consisted of hard turning shafts with cubic boron nitride (CBN) inserts, followed by burnishing with the use of various machining parameters, such as feed and force. The research focused on the examination of burnished surfaces, which was conducted for various structures after hard turning, and with variable burnishing parameters. The results obtained for the decrease of roughness are presented as the relation between the parameters Rat/Rab, which is approximately 2, while for Rpkt/Rpkb, it is around 3.7, respectively. Sat/Sab is around 2, while Spkt/Spkb is around 3.5 (where an index denotes the t-surface after turning, and the index b-surface after burnishing). The structure of the surface after burnishing and turning is described with roughness parameters, as well as with the photographs of the specimen surface, and the bearing area curve.

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